液氮+氯苯可以控制在-45度
这里有个表,看看吧
The table below gives the lowest temperature that can be obtained from a
mixture of the inorganic salt with finely shaved dry ice. With the organic
substances, dry ice (-78 摄氏度) in small lumps can be added to the
solvent until a slight excess of dry ice remains or liquid nitrogen (-196 摄
氏度) can be poured into the solvent until a slush is formed that consists
of the solid-liquid mixture at its melting point.
Substance Quantity of Quantity of Temperature,摄氏度
substance, g water, mL
Ammonium nitrate 100 94 -4.0
Sodium nitrate 75 100 -5.3
Sodium thiosulfate 5-water 110 100 -8.0
Sodium chloride 36 100 -10.0
Sodium nitrate 50 100 -17.8
Sodium bromide 66 100 -28
Magnesium chloride 85 100 -34
Calcium chloride 6-water 100 81 -40.3
100 70 -55
Ethylene glycol -13 Acetone -77
1,2-Dichlorobenzene -17 Ethyl acetate -84
Carbon tetrachloride -22.9 2-Butanone -87
Bromobenzene -31 Hexane -95
Methoxybenzene -37 Methanol -98
Bis(2-ethoxyethyl) ether -44 Carbon disulfide -112
Chlorobenzene -45 Bromoethane -119
N-Methylaniline -57 Pentane -130
p-Cymene -68 2-Methylbutane -160
【 在 linak (metallica) 的大作中提到: 】
: 上次有人说用氯化镁加冰,试了试
: 开始没注意,拿了个6个结晶水的氯化镁来试,感觉很艰难的才能降到零下27度左
: 右,主要是氯化镁一加到冰上去的时候马上就产生很多水,把水吸出去吧,感觉
: 盐好像也被弄出去了。很不好控制温度,开始以为是结晶水的原因,后来用无水
: 氯化镁,居然更难了,也就零下10度
: 做过的ggjj给出个主意吧,就这样都这么难控制,做反应的时候岂不是更不爽了
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FROM 10.22.93.12